N-芴甲氧羰基-L-赖氨酸合成路线 (共 24 条)
反应条件
tin(IV) chloride in ethyl acetate 0.416667 h; Ambient temperature;
参考文献
Chemical Communications, , # 22 p. 2509 - 2510
反应条件
trifluorormethanesulfonic acid; 3-methyl-phenol; trifluoroacetic acid T=4°C; 1 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 48, # 8 p. 1230 - 1233
反应条件
lithium hydroxide in tetrahydrofuran; water T=0°C; 0.0833333 h;
参考文献
Tetrahedron, , vol. 61, # 9 p. 2493 - 2503
反应条件
porcine pancreas trypsin type IX-S; sodium hydrogencarbonate in ethanol; water T=37°C; pH=8.3; 30 h; aq. bufferEnzymatic reaction;
参考文献
Tetrahedron, , vol. 66, # 14 p. 2614 - 2618
反应条件
porcine pancreas trypsin type IX-S; sodium hydrogencarbonate in water-d2; methanol-d4 T=37°C; pH=8.3; 30 h; aq. bufferEnzymatic reaction;
参考文献
Tetrahedron, , vol. 66, # 14 p. 2614 - 2618
反应条件
1: With sodium carbonate in water; acetonitrile T=0 - 20°C; pH=8; 2: With potassium hydrogensulfate in water; acetonitrile pH=2 - 3;
参考文献
Synthetic Communications, , vol. 39, # 11 p. 2022 - 2031
反应条件
1: 88 percent / trifluoroacetic acid / CH2Cl2 / 3 h / 20 °C 2: 69 percent / N,N-diisopropylethylamine / CH2Cl2 / 0 - 20 °C 3: LiOH / tetrahydrofuran; H2O / 0.08 h / 0 °C View Scheme
参考文献
Tetrahedron, , vol. 61, # 9 p. 2493 - 2503
反应条件
1: 69 percent / N,N-diisopropylethylamine / CH2Cl2 / 0 - 20 °C 2: LiOH / tetrahydrofuran; H2O / 0.08 h / 0 °C View Scheme
参考文献
Tetrahedron, , vol. 61, # 9 p. 2493 - 2503
反应条件
in acetonitrile T=20°C; pH=9.2; 0.25 h; aq. borate buffer;
参考文献
Journal of the Chinese Chemical Society, , vol. 58, # 4 p. 509 - 515
反应条件
in tetrahydrofuran; acetic anhydride T=20°C;
参考文献
Hughes, Robert M.; Waters, Marcey L.
Journal of the American Chemical Society, 2006 , vol. 128, # 41 p. 13586 - 13591