N-芴甲氧羰基-L-赖氨酸合成路线 （共 24 条）
反应条件
sodium azide in N,N-dimethyl-formamide T=50°C; 4 h;
参考文献
Chen, Chun-Chi; Rajagopal, Basker; Liu, Xuan Yu; Chen, Kuan Lin; Tyan, Yu-Chang; Lin, Fui; Lin, Po-Chiao
Amino Acids, 2014 , vol. 46, # 2 p. 367 - 374
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=20°C; 0.333333 h;
参考文献
Hughes, Robert M.; Waters, Marcey L.
Journal of the American Chemical Society, 2006 , vol. 128, # 41 p. 13586 - 13591
反应条件
1: N-(9-fluorenylmethoxycarbonyl)-L-lysine With chloro-trimethyl-silane in dichloromethane T=20 - 50°C; 1 h; Heating / reflux; 2: diphenyl-(4-methoxyphenyl)-methyl chloride With N-ethyl-N,N-diisopropylamine in dichloromethane T=0 - 20°C;
参考文献
Weinshenker, Ned M.; West, Frederick G.; Araneo, Barbara A.; Li, Weiping
Patent: US2005/54607 A1, 2005 ;
Location in patent: Page/Page column 17 ;
反应条件
1: With potassium carbonate in 1,4-dioxane; water T=23°C; 20 h; 2: With hydrogenchloride in water
参考文献
Klar, Ulrich; Willuda, Joerg; Menrad, Andreas; Bosslet, Klaus
Patent: US2005/234247 A1, 2005 ;
Location in patent: Page/Page column 15 ;
反应条件
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide T=20°C; 1 h;
参考文献
Feng, Siliang; Li, Senhao; Kang, Xiaoyu; Liu, Keliang
Journal of Chemical Research, 2010 , # 6 p. 348 - 350
反应条件
sodium hydroxide in 1,4-dioxane T=20°C;
参考文献
Wang, Jun; Uttamchandani, Mahesh; Li, Ping Sun; Yao, Shao Q.
Chemical Communications, 2006 , # 7 p. 717 - 719
反应条件
imidazole-1-sulfonyl azide hydrochloride; CuSO4‵5H2O; potassium carbonate in methanol; water 5 h;
参考文献
Byrne, Cillian; McEwan, Paul A.; Emsley, Jonas; Fischer, Peter M.; Chan, Weng C.
Chemical Communications, 2011 , vol. 47, # 9 p. 2589 - 2591
反应条件
sodium hydrogencarbonate; copper(II) sulfate in methanol; water T=20°C; pH=8 - 9;
参考文献
Galibert, Mathieu; Renaudet, Olivier; Dumy, Pascal; Boturyn, Didier
Angewandte Chemie - International Edition, 2011 , vol. 50, # 8 p. 1901 - 1904
反应条件
trifluoroacetic acid in ethanol 60 h; Heating;
参考文献
Chhabra, Siri Ram; Hothi, Bhupinder; Evans, David J.; White, Peter D.; Bycroft, Barrie W.; Chan, Weng C.
Tetrahedron Letters, 1998 , vol. 39, # 12 p. 1603 - 1606
参考文献
Bycroft, Barrie W.; Chan, Weng C.; Chhabra, Siri Ram; Hone, Neal D.
Journal of the Chemical Society, Chemical Communications, 1993 , # 9 p. 778 - 779
