1-丁氧基-4-甲基-苯合成路线 (共 17 条)
反应条件
aluminum oxide; potassium fluoride; copper(l) iodide; 1,10-phenanthroline T=110°C; 9 h;
参考文献
Hosseinzadeh, Rahman; Tajbakhsh, Mahmood; Mohadjerani, Maryam; Alikarami, Mohammad
Synlett, 2005 , # 7 art. no. D28904ST, p. 1101 - 1104
反应条件
sodium hydroxide; tetrabutylammomium bromide in hexane 2 h; Heatingeffect of catalysts and reaction times; Product distributionKinetics;
参考文献
Motoi, Masatoshi; Shimamura, Katsuhiko; Shimamura, Chikako; Muramoto, Satoru; Kanoh, Shigeyoshi; Suda, Hiroshi
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 8 p. 2553 - 2561
反应条件
5-(di(adamantan-1-yl)phosphino)-1′,3′,5′-triphenyl-1′H-1,4′-bipyrazole; palladium diacetate; caesium carbonate in toluene T=80°C; 3 h; Inert atmosphere;
参考文献
Gowrisankar, Saravanan; Sergeev, Alexey G.; Anbarasan, Pazhamalai; Spannenberg, Anke; Neumann, Helfried; Beller, Matthias
Journal of the American Chemical Society, 2010 , vol. 132, # 33 p. 11592 - 11598
反应条件
2,6-dimethylpyridine; tetrabutyl-ammonium chloride; potassium carbonate in water 8 h; Heating;
参考文献
Aki, Shinji; Nishi, Takao; Minamikawa, Jun-Ichi
Chemistry Letters, 2004 , vol. 33, # 7 p. 940 - 941
反应条件
hydrogen; Lindlar's catalyst in ethanol
参考文献
Bunina-Krivorukova,L.I. et al.
Journal of Organic Chemistry USSR (English Translation), 1970 , vol. 6, p. 996 - 999
Zhurnal Organicheskoi Khimii, 1970 , vol. 6, # 5 p. 991 - 995
反应条件
1: K2CO3 / acetone / 5 h / 95 °C 2: H2 / Pd/CaCO3 / ethanol View Scheme
参考文献
Bunina-Krivorukova,L.I. et al.
Journal of Organic Chemistry USSR (English Translation), 1970 , vol. 6, p. 996 - 999
Zhurnal Organicheskoi Khimii, 1970 , vol. 6, # 5 p. 991 - 995
反应条件
boron trifluoride in tetrachloromethane T=152°C;
参考文献
Romadan,I.A.; Weinberg,M.M.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, # 5 p. 1538 - 1543,1547 - 1551
反应条件
sodium hydroxide; chloroform in water; benzene Heating; Yields of byproduct given;
参考文献
Yonovich, Minda; Sasson, Yoel
Tetrahedron Letters, 1980 , vol. 21, p. 1875 - 1876
反应条件
caesium carbonate T=110°C; 0.333333 h; Microwave irradiationNeat (no solvent);
参考文献
Blint, Erika; Greiner, Istvan; Keglevich, Gyrgy
Letters in Organic Chemistry, 2011 , vol. 8, # 1 p. 22 - 27
参考文献
Bogert; Hamann
Am. Perfumer, 1930 , vol. 25, p. 19,75
Full Text Show Details
Patel; Nargund
Journal of the University of Bombay, Science: Physical Sciences, Mathematics, Biological Sciences and Medicine, 1946 , vol. 15/3 A, p. 31,32