3-溴四氢-2H-吡喃-2-甲腈合成路线 （共 6 条）
反应条件
1: Br2 / CCl4 / 1.) -6 to -12 deg C, 2.) room temp., 1.5 h 2: CCl4 / 16 h / Heating View Scheme
参考文献
Song, Song; Zhu, Shou-Fei; Pu, Liu-Yang; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6072 - 6075
Angew. Chem., 2013 , vol. 125, # 23 p. 6188 - 6191
反应条件
in tetrachloromethane 16 h; Heating;
参考文献
Hoffmann, H. M. R.; Giesel, Kunibert; Lies, Reinhard; Ismail, Zeinhom M.
Synthesis, 1986 , # 7 p. 548 - 551
反应条件
in tetrachloromethane 16 h; Reflux;
参考文献
Song, Song; Zhu, Shou-Fei; Pu, Liu-Yang; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6072 - 6075
Angew. Chem., 2013 , vol. 125, # 23 p. 6188 - 6191
反应条件
1: piperidine / 60.5 h / 20 - 30 °C 2: potassium hydroxide / water / 12 h 3: caesium carbonate; hydrogen; C63H78IrNOP(2+)*C32H12BF24(1-) / methanol / 12 h / 60 °C / 4560.31 Torr / |Autoclave View Scheme
参考文献
Song, Song; Zhu, Shou-Fei; Pu, Liu-Yang; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6072 - 6075
Angew. Chem., 2013 , vol. 125, # 23 p. 6188 - 6191
反应条件
piperidine in tetrachloromethane 60 h; Ambient temperature; Yield given;
参考文献
Hoffmann, H. M. R.; Giesel, Kunibert; Lies, Reinhard; Ismail, Zeinhom M.
Synthesis, 1986 , # 7 p. 548 - 551
反应条件
1: piperidine / CCl4 / 60 h / Ambient temperature 2: KOH / H2O / 24 h / Heating View Scheme
参考文献
Song, Song; Zhu, Shou-Fei; Pu, Liu-Yang; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6072 - 6075
Angew. Chem., 2013 , vol. 125, # 23 p. 6188 - 6191
