2-(2-溴乙酰基)噻吩合成路线 （共 37 条）
反应条件
1: 61 percent / dimethylformamide / 1.5 h / Heating 2: 82 percent / NH2NH2 / dimethylformamide / 2 h / Heating View Scheme
参考文献
Romanenko, N. I.; Fedulova, I. V.; Priimenko, B. A.; Samura, B. A.; Kapkan, L. M.; et al.
Pharmaceutical Chemistry Journal, 1986 , vol. 20, # 4 p. 253 - 256
Khimiko-Farmatsevticheskii Zhurnal, 1986 , vol. 20, # 4 p. 427 - 430
反应条件
1: 61 percent / dimethylformamide / 1.5 h / Heating 2: 75 percent / dimethylformamide / 2 h / Heating View Scheme
参考文献
Romanenko, N. I.; Fedulova, I. V.; Priimenko, B. A.; Samura, B. A.; Kapkan, L. M.; et al.
Pharmaceutical Chemistry Journal, 1986 , vol. 20, # 4 p. 253 - 256
Khimiko-Farmatsevticheskii Zhurnal, 1986 , vol. 20, # 4 p. 427 - 430
反应条件
1: 61 percent / dimethylformamide / 1.5 h / Heating 2: 79 percent / dimethylformamide / 2 h / Heating View Scheme
参考文献
Romanenko, N. I.; Fedulova, I. V.; Priimenko, B. A.; Samura, B. A.; Kapkan, L. M.; et al.
Pharmaceutical Chemistry Journal, 1986 , vol. 20, # 4 p. 253 - 256
Khimiko-Farmatsevticheskii Zhurnal, 1986 , vol. 20, # 4 p. 427 - 430
参考文献
Brunswig
Chemische Berichte, 1886 , vol. 19, p. 2893
反应条件
sodium amide; triethyl phosphite 1.) 90 deg C, 1,5h, 2.) ether, -78 deg C, 1h; Yield given. Multistep reaction;
参考文献
Kagan, Jaques; Arora, Sudershan K.; Bryzgis, Marius; Dhawan, Som N.; Reid, Kevin; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 5 p. 703 - 706
反应条件
potassium hydroxide in ethanol 1 h; Heating;
参考文献
Smirnov, V. A.; Zimichev, A. V.; Lyzhova, G. A.; Lipkin, A. E.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 1 p. 28 - 31
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 1 p. 35 - 38
反应条件
1: 75 percent / ethanol / 1 h / Heating 2: 8 percent / diethyl ether; tetrahydrofuran / 6 h / Irradiation View Scheme
参考文献
Hesabi, Massoud M.; Hill, John; El-Hamamy, Ahmad A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2371 - 2373
反应条件
1-methyl-1H-imidazole in water; isopropyl alcohol T=20°C; 1.5 h;
参考文献
Meshram; Thakur, Pramod B.; Madhu Babu; Bangade, Vikas M.
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5265 - 5269
反应条件
in ethanol 2 h; Heating;
参考文献
Farag, Ahmed M.; Hassaneen, Hamdi M.; Abbas, Ikhlas M.; Shawali, Ahmad S.; Algharib, Mohamad S.
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 40, p. 243 - 250
反应条件
in methanol 2.5 h; Heating;
参考文献
Spirkova, Katarina; Bobal, Pavel; Dandarova, Miloslava; Alfoldi, Juraj
Collection of Czechoslovak Chemical Communications, 1992 , vol. 57, # 10 p. 2157 - 2165
