2,3,3A,4,7,7a-六氢-1H-异吲哚合成路线 （共 3 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 35 h; RefluxInert atmosphere;
参考文献
Anastasiadis, Charalampos; Hogarth, Graeme; Wilton-Ely, James D.E.T.
Inorganica Chimica Acta, 2010 , vol. 363, # 13 p. 3222 - 3228
反应条件
1: dichloromethane / 21.5 h / 0 - 20 °C 2: sodium periodate; ruthenium(IV) oxide / acetonitrile; water; tetrachloromethane / 24 h / 20 °C 3: sodium acetate; acetic anhydride / 3 h / 120 °C View Scheme
参考文献
XI, Ning; WANG, Tingjin; YI, Lei
Patent: WO2013/138210 A1, 2013 ;
反应条件
1: dichloromethane / 21.5 h / 0 - 20 °C
2: sodium periodate; ruthenium(IV) oxide / acetonitrile; water; tetrachloromethane / 24 h / 20 °C
3: sodium acetate; acetic anhydride / 3 h / 120 °C
4: sodium tetrahydroborate; ethanol / 4.5 h / 20 °C
View Scheme
参考文献
XI, Ning; WANG, Tingjin; YI, Lei
Patent: WO2013/138210 A1, 2013 ;
