in acetonitrile
byproducts: NH2(CH3)2Cl; addn. of excess of NH(CH3)2 at -78°C for 2 h, then 8 h reflux; crystd. from light petroleum; elem. anal.;
参考文献
Kilic, Zeynel; Guenduez, Necla; Kilic, Emine; Nazir, Hasan
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1989 , vol. 19, p. 453 - 468
in diethyl ether
byproducts: NH2(CH3)2Cl; addn. of excess of NH(CH3)2 at -78°C for 2 h, then 8 h reflux; crystn.; elem. anal.;
参考文献
Kilic, Zeynel; Guenduez, Necla; Kilic, Emine; Nazir, Hasan
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1989 , vol. 19, p. 453 - 468
