1-(3,4-二甲氧基苯基)-2-(2-甲氧基苯基)-丙烷-1,3-二醇合成路线 （共 41 条）
反应条件
sodium tetrahydroborate in tetrahydrofuran; water T=20°C;
参考文献
Nguyen, John D.; Matsuura, Bryan S.; Stephenson, Corey R. J.
Journal of the American Chemical Society, 2014 , vol. 136, # 4 p. 1218 - 1221
反应条件
1: dimethylformamide 2: LiAlH4 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 27, p. 2111 - 2114
反应条件
1: Br2 / CHCl3 2: dimethylformamide 3: LiAlH4 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 27, p. 2111 - 2114
反应条件
lithium aluminium tetrahydride
参考文献
Journal of Organic Chemistry, , vol. 27, p. 2111 - 2114
反应条件
sodium tetrahydroborate
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 1403 - 1404
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1511 - 1512
反应条件
1: K2CO3 2: NaBH4 View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 1403 - 1404
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1511 - 1512
反应条件
1: K2CO3 2: K2CO3 3: NaBH4 View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 1403 - 1404
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1511 - 1512
反应条件
1: K2CO3 2: K2CO3 3: NaBH4 View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 1403 - 1404
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1511 - 1512
反应条件
1: hydrogenchloride / ethanol / 3 h / 60 °C 2: sulfur trioxide pyridine complex; triethylamine / dimethyl sulfoxide; dichloromethane / 20 °C 3: formic acid; [Ir(phenylpyridine(-1H))2(4,4′-di-tert-butyl-2,2′-bipyridine)](PF6); N-ethyl-N,N-diisopropylamine / acetonitrile / 24 h / 20 °C / |Irradiation View Scheme
参考文献
Nguyen, John D.; Matsuura, Bryan S.; Stephenson, Corey R. J.
Journal of the American Chemical Society, 2014 , vol. 136, # 4 p. 1218 - 1221
反应条件
isopropyl alcohol in ethyl acetate T=100°C; 24 h; Overall yield = > 95 percentSpectr.;
参考文献
KAT2BIZ AB; SAMEC, Joseph; GALKIN, Maxim
Patent: WO2014/38989 A1, 2014 ;
Location in patent: Page/Page column 5 ;
