双(五氟苯基)二甲基硅烷合成路线 （共 21 条）
反应条件
in diethyl ether reaction at -78°C, heating to 20°C, 12 hours;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 1.3.3.7, page 17 - 32
反应条件
phosphorous acid trisdiethylamide in pentane
参考文献
Journal of Fluorine Chemistry, , vol. 53, # 2 p. 213 - 231
反应条件
in diethyl ether heating 48 hours;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 4.1, page 147 - 165
反应条件
in diethyl ether reaction under reflux, 24 hours;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 2.2.4, page 68 - 115
反应条件
in tetrahydrofuran addition of a 10 fold excess of C6F5Li under stirring, reaction at -65°C;;
参考文献
Journal of Organometallic Chemistry, , vol. 13, p. 257
反应条件
in diethyl ether reaction at -79°C (1 hour), heating to 20°C (8 hours), heating under reflux for 2 hours; further products;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 1.3.3.7, page 17 - 32
反应条件
(i) nBuLi, Et2O, (ii) /BRN= 605287/; Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 11, p. 463 - 469
反应条件
(i) nBuLi, (ii) /BRN= 2036592/; Multistep reaction;
参考文献
Chemische Berichte, , vol. 104, p. 2124 - 2133
反应条件
XeF2; cesium fluoride in acetonitrile T=10 - 20°C; 0.5 h;
参考文献
Bardin, V. V.; Stennikova, I. V.; Furin, G. G.; Leshina, T. V.; Yakobson, G. G.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 11 p. 2580 - 2588,2297 - 2303
反应条件
XeF2; cesium fluoride in acetonitrile T=10 - 20°C; 0.333333 h;
参考文献
Bardin, V. V.; Stennikova, I. V.; Furin, G. G.; Leshina, T. V.; Yakobson, G. G.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 11 p. 2580 - 2588,2297 - 2303
