T=90°C; 4 h;

triethylamine in benzene

<b>Multi-step reaction with 2 steps<br /> </b>1: hydroxylamine hydrochloride; sodium acetate / methanol; water / 12 h / 20 &deg;C<br />2: N-chloro-succinimide / N,N-dimethyl-formamide / 5 h / 20 &deg;C<br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '113915', constants.ctx, '0')">N-chloro-succinimide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br />T=35&deg;C;&nbsp;&nbsp;Cooling with ice;&nbsp;<br /> <br /> &nbsp;