1,2,3,4,5,6,7,8-八硫杂环辛烷合成路线 （共 272 条）
反应条件
in carbon disulfide Kinetics; byproducts: S5, S9; Irradiation (UV/VIS); photolysis (high pressure Hg lamp, 200-600 nm), 15°C; monitoring by HPL chromy.;
参考文献
Zeitschrift fuer Naturforschung, B: Chemical Sciences, , vol. 42, # 6 p. 682 - 690
反应条件
in neat (no solvent) dry box; dissolving Se in S2Cl2 (1-3 h); further products; not isolated; detn. by Raman- and (77)Se-NMR spectroscopy;
参考文献
Canadian Journal of Chemistry, , vol. 70, # 3 p. 693 - 699
反应条件
in neat (no solvent) educt sealed under Ar heated at heating rate of 7.5 K/min up to 423-443 K; solid dissolved in CCl4, identified by TLC and with gas chromatograph;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 7 p. 2391 - 2394
反应条件
in neat (no solvent) Kinetics; Sonication; 20 kHz, 0°C, N2 atm.; GS/MS;
参考文献
Zeitschrift fur Anorganische und Allgemeine Chemie, , vol. 622, # 2 p. 259 - 261
反应条件
in dichloromethane Irradiation (UV/VIS); soln. decolourised in ca. 30 min.;;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1343 - 1346
反应条件
in acetonitrile byproducts: (Ph2PN)3*HCl, 1,5-(Ph2PN)2(SN)2, Ph2P(S)Cl; ligand was added to stirred soln. of CsS3N3 in CH3CN at 23°C for38 h; filtered off, solvent was removed in vac., isolated by fractional crystn.;
参考文献
Canadian Journal of Chemistry, , vol. 61, p. 1957 - 1962
反应条件
slow decompn. in soln. and in the solid state at room temp. and even at -55°C;
参考文献
Organometallics, , vol. 21, # 13 p. 2604 - 2608
反应条件
in water prepn. mechanochemically; FeS was activated using vibration mill; O2 atm.; steel reactor; time - 5 h; 20°C;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 53, # 7 p. 981 - 987
反应条件
in neat (no solvent) prepn. mechanochemically; FeS2 was activated using vibration mill; O2 atm.; steel reactor; time - 5 h; 20°C;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 53, # 7 p. 981 - 987
反应条件
in dichloromethane; acetonitrile High Pressure; Schlenk techniques; mixing Cu compd., S compd. in CH2Cl2/MeCN, sealing in autoclave, heating at 90°C for 20 h;
参考文献
Dalton Transactions, , vol. 40, # 4 p. 847 - 852
