1,2,3,4,5,6,7,8-八硫杂环辛烷合成路线 （共 272 条）
反应条件
in neat (no solvent) a solid sample was allowed to warm to 20°C;
参考文献
Zeitschrift fuer Naturforschung, B: Chemical Sciences, , vol. 44, # 12 p. 1499 - 1502
反应条件
in water prepn. mechanochemically; FeS2 was activated using vibration mill; O2 atm.; steel reactor; time - 5 h; 20°C;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 53, # 7 p. 981 - 987
反应条件
in ethanol; water High Pressure; mixt. of Cu-salt and (C5H4NS)2 (1:1 molar ratio) in H2O/C2H5OH in sealedvessel heated to 140°C in microwave oven within 20 min (300 W), temp. kept for 1 h, vessel slowly cooled to room temp within 8 h; orange crystals of Cu6(C5H4NS)6 and yellow crystals of Cu(I)-Cu6(II) complex salt sepd., washed with ethanol and dried in air, filtrate stored at 0°C for 2 weeks, crystals of Cu2 complex and S8 isolated; elem.anal.;
参考文献
Dalton Transactions, , vol. 39, # 9 p. 2280 - 2287
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 260, p. 273 - 278
S: SVol.4a/b, 2.2.3.5, page 421 - 421
反应条件
potassium iodide byproducts: I2, S18, S20; 25°C; chromy.;
参考文献
Angewandte Chemie, , vol. 93, p. 402 - 404
反应条件
potassium iodide byproducts: I2, S18, S20; 25°C; chromy.;
参考文献
Angewandte Chemie, , vol. 93, p. 402 - 404
反应条件
in carbon disulfide N2-atmosphere, refluxing (46°C) for 3 h; extn. with CS2, concn. of extract, chromy. (Bio Beads S-X8, CS2), evapn., IR spectroscopy;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 234 - 237
反应条件
byproducts: polymer sulfur; at 25°C;
参考文献
Angewandte Chemie, International Edition in English, , vol. 15, p. 772 - 773
Angewandte Chemie, , vol. 88, p. 854 - 855
S: SVol.3, 1.4, page 8 - 10
参考文献
Angewandte Chemie, International Edition in English, , vol. 17, p. 611 - 612
Angewandte Chemie, , vol. 90, p. 644 - 645
S: SVol.3, 1.5, page 10 - 11
参考文献
Angewandte Chemie, International Edition in English, , vol. 17, p. 611 - 612
Angewandte Chemie, , vol. 90, p. 644 - 645
S: SVol.3, 1.5, page 10 - 11
