1,2,3,4,5,6,7,8-八硫杂环辛烷合成路线 （共 272 条）
反应条件
in carbon disulfide byproducts: S9; in a sealed ampoule; 130-155°C; quenched with ice-water; HPLC;
参考文献
Tebbe, Fred N.; Wasserman, E.; Peet, William G.; Vatvars, Arturs; Hayman, Alan C.
Journal of the American Chemical Society, 1982 , vol. 104, p. 4971 - 4972
反应条件
in carbon disulfide Kinetics; byproducts: cyclo-S5, S9; Irradiation (UV/VIS); photolysis (high-pressure Hg lamp, 200-600 nm), 15°C; monitoring by HPL chromy.;
参考文献
Strauss, Eva-Maria; Steudel, Ralf
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1987 , vol. 42, # 6 p. 682 - 690
反应条件
carbon in neat (no solvent) byproducts: CO2, CS2; thermal analysis of black powder; heating of black powder up to 500°C under various conditions; DSC, TG, TG-DTA-FTIR-MS, ARC, HFC;
参考文献
Turcotte; Fouchard; Jones
Journal of Thermal Analysis and Calorimetry, 2003 , vol. 73, # 1 p. 105 - 118
反应条件
3-fold excess of S8;
参考文献
Schmidt, M.; Schumann, H.
Chemische Berichte, 1963 , vol. 96, p. 462 - 464
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.16.1.4.3, page 156 - 157
反应条件
in benzene To stibane compound in benzene is added S8, cooling of mixture with cold water and stirring for 0.5 h under Ar.; removal of solvent under vac., distn., elem. anal.;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 44, p. 129 - 134
参考文献
Datta, J.
Journal of the Indian Chemical Society, 1952 , vol. 29, p. 101 - 104
Full Text Show Details
Datta, J.
Journal of the Indian Chemical Society, 1952 , vol. 29, p. 965
Full Text Show Details
Gmelin Handbook: S: SVol.4a/b, 1.1.2, page 11 - 12
反应条件
heating with dry metal hydroxide above 235°C; formation of pure H2S;
参考文献
Datta, J.
Journal of the Indian Chemical Society, 1952 , vol. 29, p. 101 - 104
Full Text Show Details
Datta, J.
Journal of the Indian Chemical Society, 1952 , vol. 29, p. 965
Full Text Show Details
Gmelin Handbook: S: SVol.4a/b, 1.1.2, page 11 - 12
反应条件
in toluene byproducts: H2; Ar atmosphere, stirring (80-90°C, 8 h); washing (pentane), drying (0.1 Torr);
参考文献
Chemische Berichte, , vol. 121, p. 709 - 722
反应条件
in solid Cu and S8 were mixed, heated at 46-450°C; study of influence of:mechanical treatment, mixing with a spatula, pressure (0.12-1.38 GPa), milling time (1-120 min), particle size of copper (32-112 μm), ageing, heating rate (1-40 K/min); detected by X-ray diffraction;
参考文献
Hyett, Geoffrey; Barrier, Nicolas; Clarke, Simon J.; Hadermann, Joke
Journal of the American Chemical Society, 2007 , vol. 129, # 36 p. 11192 - 11201
反应条件
in neat (no solvent) mortaring of Cu(3-x)As and S8, flushing of quartz ampoules with Ar, filling with this mixt., sealing, heating up to 680°C with a rate of 10 K/min, quenching; identification by X-ray diffraction;
参考文献
Mueller; Blachnik
Thermochimica Acta, 2002 , vol. 387, # 2 p. 153 - 171
