1,2,3,4,5,6,7,8-八硫杂环辛烷合成路线 （共 272 条）
反应条件
in methanol slow react. at 4.5°C;;
参考文献
Bartlett, P. D.; Davis, R. E.
Journal of the American Chemical Society, 1958 , vol. 80, p. 2513 - 2516
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Gmelin Handbook: Na: SVol.4, 9, page 1387 - 1389
反应条件
in tetrachloromethane reduction of S4N4 with aq. hydrazine and S8 in CCl4 as solvent (furtherinert solvents are possible); further products; evapn. of solvent, isolation by chromy. (silica gel or polystyrene gel);
参考文献
Garcia-Fernandez, H.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 28, p. 3 - 20
反应条件
in tetrachloromethane reduction of S4N4 with aq. hydrazine and S8 in CCl4 as solvent (furtherinert solvents are possible); further products; evapn. of solvent, isolation by chromy. (silica gel or polystyrene gel);
参考文献
Garcia-Fernandez, H.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 28, p. 3 - 20
反应条件
pyridine in pyridine to NaBH4 in a flask at 10°C is added pyridine, then is slowly added sulfur (2 h); the amine is evapd., to the residue is added benzene, the solvent is after 1 d removed, elem. anal.;
参考文献
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, , vol. 38, # 2 p. 203 - 207
反应条件
NH3 in ammonia NH3 (liquid); inert atmosphere;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1179 - 1186
反应条件
in pyridine react. of copper powder and S8 in refluxing pyridine; PXRD;
参考文献
Ramli, Emannuel; Rauchfuss, Thomas B.; Stern, Charlotte L.
Journal of the American Chemical Society, 1990 , vol. 112, # 10 p. 4043 - 4044
反应条件
in liquid sulphur dioxide C2F4, SbF5 and S8 molar ratio = 2.5:1, in autoclave at 20°C, 6 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
反应条件
NH3 in ammonia NH3 (liquid); inert atmosphere;
参考文献
O'Mahoney, Caroline A.; Parkin, Ivan P.; Williams, David J.; Woollins, J. Derek
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1989 , p. 1179 - 1186
反应条件
in neat (no solvent, solid phase) high temp.;
参考文献
Inorganic Chemistry, , vol. 51, # 10 p. 5839 - 5843
反应条件
in further solvent(s) (N2); sulfur added slowly to cooled (0°C) hydrazine monohydrate in air; filtered under gravity; ppt. filtered off; washed (water, isopopyl alcohol); dried; fired under inert atm. at 700°C;
参考文献
Journal of the Electrochemical Society, , vol. 147, # 2 p. 765 - 771
