1,2,3,4,5,6,7,8-八硫杂环辛烷合成路线 （共 272 条）
反应条件
diethylamine in acetone
to NaBH4 in a flask is added a mixt. of acetonitrile and Et2NH, then slowly sulfur is added (15 h, 45°C); amine and acetone are removed, elem. anal.;
参考文献
Binder, Herbert; Diamantikos, Wassilios
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1983 , vol. 38, # 2 p. 203 - 207
反应条件
NH3 in ammonia
NH3 (liquid); inert atmosphere;
参考文献
O'Mahoney, Caroline A.; Parkin, Ivan P.; Williams, David J.; Woollins, J. Derek
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1989 , p. 1179 - 1186
反应条件
in pentane
Ar atmosphere, stirring (0°C, 1 h; 20°C, 2 h), sepn. of Me3PS (filtration off); crystn. on cooling (dry ice); elem. anal.;
参考文献
Klein, Hans-Friedrich; Gass, Michael; Koch, Udo; Eisenmann, Brigitte; Schaefer, Herbert
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1988 , vol. 43, # 7 p. 830 - 838
反应条件
in benzene
Ar atmosphere; stirring (ambient temp., 10 min); filtration;
参考文献
Barrau, Jacques; Hamida, Najib Ben; Satge, Jacques
Journal of Organometallic Chemistry, 1990 , vol. 387, # 1 p. 65 - 76
参考文献
Genz, W.; Schenk, P. W.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1970 , vol. 379, p. 300 - 311
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Murthy, A. R. V.
Proceedings - Indian Academy of Sciences, Section A, 1952 , vol. 36, p. 388 - 401
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Schenk, P. W.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1934 , vol. 220, p. 268 - 272
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Gmelin Handbook: S: SVol.3, 1.10.1, page 17 - 21
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Genz, W.
Diss. Berlin T.U. 1969
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Murthy, A. R. V.
Silicium. Schwefel. Phosphate, IUPAC Colloq. Muenster, Westf., 1954 (1955), S. 141/6
参考文献
Schenk, P. W.; Triebel, H.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1936 , vol. 229, p. 305 - 312
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Gmelin Handbook: S: SVol.3, 1.10.1, page 17 - 21
反应条件
oxygen
in mass spectrum;
参考文献
Gmelin Handbook: S: SVol.3, 1.14, page 37 - 37
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Liuti, G.; Dondes, S.; Harteck, P.
Abstr. Papers 145th Nat. Meeting Am. Chem. Soc., New York 1963, Abstr. 40T
反应条件
in tetrachloromethane
byproducts: S8; reduction of S4N4 with aq. hydrazine and S8 in CCl4 as solvent (furtherinert solvents are possible); further products;; evapn. of solvent, isolation by chromy. (silica gel or polystyrene gel);
参考文献
Garcia-Fernandez, H.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 28, p. 3 - 20
反应条件
in tetrachloromethane
reduction of S4N4 with aq. hydrazine and S8 in CCl4 as solvent (furtherinert solvents are possible); further products; evapn. of solvent, isolation by chromy. (silica gel or polystyrene gel);
参考文献
Garcia-Fernandez, H.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 28, p. 3 - 20
参考文献
Parkin, Ivan P.; Woollins, J. Derek; Belton, Peter S.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1990 , p. 511 - 518
