1,2,3,4,5,6,7,8-八硫杂环辛烷合成路线 （共 272 条）
反应条件
in benzene
heating to 50°C with an excess of sulfur; 2,4-digerma-1,3-dithietane is characterized by comparison to an authentic sample; metadithiophosphonate is characterized by NMR;
参考文献
Andrianarison, Mbolatiana; Couret, Claude; Declercq, Jean-Paul; Dubourg, Antoine; Escudie, Jean; et al.
Organometallics, 1988 , vol. 7, p. 1545 - 1548
反应条件
diethylamine in ethanol
T=20°C; 1 h;
参考文献
DEVELOGEN AKTIENGESELLSCHAFT
Patent: WO2006/136402 A1, 2006 ;
Location in patent: Page/Page column 104 ;
WO 2006/136402 A1
反应条件
in not given
byproducts: H2S;
参考文献
Vyazankin, N. S.; Bochkarev, M. N.; Sanina, L. P.
Zhurnal Obshchei Khimii, 1966 , vol. 36, p. 166 - 166
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.2.4.4, page 32 - 34
参考文献
Ponomarev, S. V.; Lutsenko, I. F.
Zhurnal Obshchei Khimii, 1964 , vol. 34, p. 3450 - 3453
C. A., 1965 , vol. 62, p. 2787
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.2.2, page 162 - 181
反应条件
in further solvent(s)
in SbF5, 70°C, 1 h;
参考文献
Yakobson, G. G.; Furin, G. G.; Terent'eva, T. V.
Zhurnal Organicheskoi Khimii, 1974 , vol. 10, p. 802 - 806
Zhurnal Organicheskoi Khimii, 1974 , vol. 10, p. 799 - 804
反应条件
in tetrachloromethane
reduction of S4N4 with aq. hydrazine and S8 in CCl4 as solvent (furtherinert solvents are possible); further products; evapn. of solvent, isolation by chromy. (silica gel or polystyrene gel);
参考文献
Garcia-Fernandez, H.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 28, p. 3 - 20
反应条件
anatase O2Ti in sodium hydroxide
Kinetics; byproducts: S(2-), S2O3(2-), SO3(2-); Irradiation (UV/VIS); also in water, with or without catalyst, with anatase or rutile, also in presence of N2, with or without filter, for 1 h; yield depending on time; concentration of byproducts depending on catalyst and conditions;
参考文献
Matsumoto, Yasumichi; Nagal, Hideaki; Sato, Ei-ichi
Journal of Physical Chemistry, 1982 , vol. 86, # 24 p. 4664 - 4668
反应条件
(N2), bomb reed, heated at 182°C for 4 h; cooled in liquid air in vac., distd.;
参考文献
Schmidt, M.; Froehlich, B.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1987 , vol. 553, p. 239 - 247
参考文献
Schmidt, M.; Siebert, W.; Gast, E.
Zeitschrift fuer Naturforschung, 1967 , vol. 22b, p. 557 - 558
参考文献
Davy, H.
Annales de Chimie (Cachan, France), 1813 , vol. 88, p. 327
Full Text Show Details
Gay-Lussac, L. J.
Annales de Chimie (Cachan, France), 1813 , vol. 88, p. 319
