1,2,3,4,5,6,7,8-八硫杂环辛烷合成路线 （共 272 条）
反应条件
in further solvent(s)
uptake of finely pulverized S at ambient temp. slowly, on warming largely;; generation of H2S, on cooling deposition of S;;
参考文献
Bloch, I.; Hoehn, F.
Ber., 1908 , vol. 41, p. 1961 - 1971
反应条件
in ammonia
byproducts: N2; at -40°C (chromy. of vapor phase);
参考文献
Guiraud, R.; Aubry, M.
Bulletin de la Societe Chimique de France, 1977 , p. 453 - 454
Full Text Show Details
Gmelin Handbook: S: SVol.4a/b, 1.1.2, page 11 - 12
反应条件
(N2), bomb reed, heated at 182°C for 4 h; cooled in liquid air in vac., distd.;
参考文献
Schmidt, M.; Froehlich, B.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1987 , vol. 553, p. 239 - 247
反应条件
aluminium
byproducts: CH3SCH3; (N2), bomb reed, heated at 270°C for 45 h; cooled in liquid air in vac., distd.;
参考文献
Schmidt, M.; Froehlich, B.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1987 , vol. 553, p. 239 - 247
反应条件
in water
prepn. mechanochemically; S8 was activated using vibration mill; vac., Ar or air atm.; quartz ampoule; time - 1 h; room temp.;
参考文献
Pavelko
Russian Journal of Inorganic Chemistry, 2008 , vol. 53, # 7 p. 981 - 987
参考文献
Datta, J.
Journal of the Indian Chemical Society, 1952 , vol. 29, p. 101 - 104
Full Text Show Details
Datta, J.
Journal of the Indian Chemical Society, 1952 , vol. 29, p. 965
Full Text Show Details
Gmelin Handbook: S: SVol.4a/b, 1.1.2, page 11 - 12
反应条件
heating with dry metal hydroxide above 235°C; formation of pure H2S;
参考文献
Datta, J.
Journal of the Indian Chemical Society, 1952 , vol. 29, p. 101 - 104
Full Text Show Details
Datta, J.
Journal of the Indian Chemical Society, 1952 , vol. 29, p. 965
Full Text Show Details
Gmelin Handbook: S: SVol.4a/b, 1.1.2, page 11 - 12
反应条件
heating with dry metal hydroxide; formation of pure H2S;
参考文献
Datta, J.
Journal of the Indian Chemical Society, 1952 , vol. 29, p. 101 - 104
Full Text Show Details
Datta, J.
Journal of the Indian Chemical Society, 1952 , vol. 29, p. 965
Full Text Show Details
Gmelin Handbook: S: SVol.4a/b, 1.1.2, page 11 - 12
反应条件
(N2), bomb reed, heated at 145°C for 20 h; cooled in liquid air in vac., distd.;
参考文献
Schmidt, M.; Froehlich, B.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1987 , vol. 553, p. 239 - 247
反应条件
heating with dry metal hydroxide; formation of pure H2S;
参考文献
Datta, J.
Journal of the Indian Chemical Society, 1952 , vol. 29, p. 101 - 104
Full Text Show Details
Datta, J.
Journal of the Indian Chemical Society, 1952 , vol. 29, p. 965
Full Text Show Details
Gmelin Handbook: S: SVol.4a/b, 1.1.2, page 11 - 12
