1,2,3,4,5,6,7,8-八硫杂环辛烷合成路线 （共 272 条）
参考文献
B: B-Verb.3, 2.5.1.2, page 17 - 18
unveroeffentlich (1975)
参考文献
B: B-Verb.3, 2.5.1.2, page 17 - 18
unveroeffentlich (1975)
参考文献
B: B-Verb.3, 2.5.1.2, page 17 - 18
unveroeffentlich (1975)
参考文献
B: B-Verb.3, 2.5.1.2, page 17 - 18
unveroeffentlich (1975)
反应条件
other Radiation; at 25°C by green or blue Laser light;
参考文献
J. Mol. Spectrosc., , vol. 51, p. 334 - 340
反应条件
in neat (no solvent, solid phase) 20°C, 24 h;
参考文献
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, , vol. 40, # 5 p. 594 - 600
反应条件
in acetonitrile byproducts: (Ph2PN)3, 1,5-(Ph2PN)2(SN)2, Ph2P(S)Cl; ligand was added to stirred soln. of CsS3N3 in CH3CN at 0°C for 158 h; filtered off, solvent was removed in vac., chromd.;
参考文献
Canadian Journal of Chemistry, , vol. 61, p. 1957 - 1962
反应条件
in neat (no solvent) prepn. mechanochemically; FeS was activated using vibration mill; O2 atm.; steel reactor; time - 5 h; 20°C;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 53, # 7 p. 981 - 987
反应条件
in dichloromethane; acetonitrile byproducts: SO4(2-); other Radiation; mixing Cu compd., S compd. in CH2Cl2/MeCN (1:1), sealing in autoclave, irradiation in microwave oven (2*800 W, 2.45 GHz), heating to 90°Cin 20 min, storage for 1 h, various times (1 h or 3-20 h), various temp . (60 or 90°C); slow cooling to room temp. over 9 h, isolation of crystals after storageat 0°C for 2 weeks, manually separation of crystals, washing wit h Et2O, air drying, elem. anal.;
参考文献
Dalton Transactions, , vol. 40, # 4 p. 847 - 852
反应条件
in carbon disulfide Kinetics; byproducts: S5; Irradiation (UV/VIS); photolysis (high pressure Hg lamp, 200-600 nm), 15°C; monitoring by HPL chromy.;
参考文献
Zeitschrift fuer Naturforschung, B: Chemical Sciences, , vol. 42, # 6 p. 682 - 690
