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sodium tris(diethylamino)aluminum hydride in tetrahydrofuran; N-dodecane T=-78°C; 6 h;
参考文献
Cha, Jin Soon; Kim, Jong Mi; Jeoung, Min Kyoo; Kwon, Oh Oun; Kim, Eun Ju
Organic Preparations and Procedures International, 1995 , vol. 27, # 1 p. 95 - 98
in hexane Os-cluster and ligand were placed in tube with hexane, heated for 15 h at 100°C under N2; solvent and volatiles were removed in vacuo, TLC with hexane-CH2Cl2;
参考文献
Journal of the Chemical Society, Dalton Transactions, , # 6 p. 1020 - 1023
