in neat (no solvent)
byproducts: NOCl, NO2Cl, NO; passing dry N2O4 over the surface of freshly distd. PCl3 cooled at -10 °C; absortion under formation of a dark red liq.; expelling NO, N2O3, NOCl, NO2Cl and pptn. of P2O6NCl2; liquid phase contg. POCl3, P2O3Cl4 and a small amount of P4O4Cl10;; isolation of liquid products by fractionation; yield of P2O3Cl4 17 percent and of P4O4Cl10 5 percent;;
参考文献
Gmelin Handbook: P: MVol.C, 184, page 424 - 427
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Rother, E. G. F.
Diss. Muenchen 1959, S. 1/98
in neat (no solvent)
reaction at ambient temperature;;
参考文献
Thorpe, T. E.; Tutton, A. E.
Journal of the Chemical Society, 1891 , vol. 59, p. 1019 - 1029
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Gmelin Handbook: P: MVol.C, 37, page 74 - 75
in neat (no solvent)
Electric Arc; reaction by influence of arc sparks on boiling, liquid air;;
参考文献
Kanda, E.; Nomura, Y.
Science Reports of the Research Institutes, Tohoku University, Series A: Physics, Chemistry, and Metallurgy, 1953 , vol. 5, p. 1 - 7
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Gmelin Handbook: O: MVol.4, 40, page 1074 - 1077
in neat (no solvent)
disproportion of NO on a NiY-type zeolite pressed into self-supporting wafers (dehydrated and hydrated) at 313 K, NO pressure = 5000 Pa, yielding HNO2 only on the hydrated wafer; monitoring by IR spectroscopy;
参考文献
Minming, Huang; Chunhua, Yuan; Kunsong, Chen
Journal of Molecular Catalysis, 1991 , vol. 69, p. L7 - L14
Lunge, G.; Porschnew, G.
Z. Anorg. Chem., 1894 , vol. 7, p. 240 - 249
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Ramsay, W.
Journal of the Chemical Society, 1890 , vol. 57, p. 597
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Ramsay, W.
Z. phys. Ch., 1890 , vol. 5, p. 224
