(3-溴丙基)(三甲基)硅烷合成路线 （共 26 条）
反应条件
phosphorus tribromide in not given
参考文献
Sommer; Van Strien; Whitmore
Journal of the American Chemical Society, 1949 , vol. 71, p. 3056
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Gmelin Handbook: Si: MVol.C, 9, page 28 - 32
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Dow Corning Corp.
Patent: US2557802 , 1951 ;
C. A., 1952 , p. 1026
参考文献
Merrell Dow Pharmaceuticals, Inc.
Patent: US5252587 A1, 1993 ;
反应条件
lithium bromide in ethylene glycol dimethyl ether Heating;
参考文献
Urabe, Hirokazu; Kuwajima, Isao
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1140 - 1141
参考文献
Mironow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1959 , p. 1862;engl.Ausg.S.1781
反应条件
1.) addition 25 deg C, reflux 72 h, 2.) reflux 48 h; Yield given. Multistep reaction;
参考文献
Wilt, James W.
Tetrahedron, 1985 , vol. 41, # 19 p. 3979 - 4000
反应条件
1: 1.) Li / 1.) diethylether, RT, 1 h, 2.) diethylether, RT, 2h 2: 68 percent / PBr3 / diethyl ether / 0 °C View Scheme
参考文献
Maercker, Adalbert; Eckers, Mechthild; Passlack, Michael
Journal of Organometallic Chemistry, 1980 , vol. 186, # 2 p. 193 - 205
参考文献
Sommer et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 2485,2486,2488
反应条件
in benzene-d6 Kinetics; reaction studied by (1)H-NMR;
参考文献
Wilt, James W.; Lusztyk, J.; Peeran, Mehoob; Ingold, K. U.
Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 281 - 287
反应条件
aluminium trichloride
参考文献
Sommer; Van Strien; Whitmore
Journal of the American Chemical Society, 1949 , vol. 71, p. 3056
参考文献
Sommer; Van Strien; Whitmore
Journal of the American Chemical Society, 1949 , vol. 71, p. 3056
