in neat (no solvent)
byproducts: chlorotrimethylsilane; -80°C, stirring for 5 min; crystd., sepd., dried at 20°C (7mm); elem.anal.;
参考文献
Lazukina, L. A.; Kukhar, V. P.
Journal of General Chemistry USSR (English Translation), 1983 , vol. 53, p. 2018 - 2021
Zhurnal Obshchei Khimii, 1983 , vol. 53, p. 2239 - 2243
sodium hydroxide; water in Petroleum ether
byproducts: polythionic acids; alkaline hydrolsis; shaking (2 h) of SCl2 (in petroleum ether) mixed with water (free of air) in presence of NaOH; yields depending on acidity discussed;;
参考文献
Goehring, M.; Stamm, H.; Feldmann, U.
Z. Anorg. Chem., 1942 , vol. 250, p. 56 - 71
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Gmelin Handbook: S: MVol.B3, 119, page 1786 - 1788