4-[(2,4-二氯苯基)磺酰基]苯胺合成路线 （共 4 条）
反应条件
hydrogen; RaNi Ambient temperature;
参考文献
Benedetti, Pier G. De; Iarossi, Dario; Menziani, Cristina; Caiolfa, Valeria; Frassineti, Chiara; Cennamo, Carlo
Journal of Medicinal Chemistry, 1987 , vol. 30, # 3 p. 459 - 464
反应条件
1: 58 percent / EtONa / ethanol / 3 h / Heating 2: 80 percent / 85 percent m-chloroperbenzoic acid / CHCl3 / 360 h / Ambient temperature 3: 60 percent / H2 / RaNi / Ambient temperature View Scheme
参考文献
Benedetti, Pier G. De; Iarossi, Dario; Menziani, Cristina; Caiolfa, Valeria; Frassineti, Chiara; Cennamo, Carlo
Journal of Medicinal Chemistry, 1987 , vol. 30, # 3 p. 459 - 464
反应条件
1: 88 percent / Zinc, sulfuric acid / 1.) 0 deg C, 2 h, 2.) RT, 2 h, 3.) reflux, 5 h 2: 58 percent / EtONa / ethanol / 3 h / Heating 3: 80 percent / 85 percent m-chloroperbenzoic acid / CHCl3 / 360 h / Ambient temperature 4: 60 percent / H2 / RaNi / Ambient temperature View Scheme
参考文献
Benedetti, Pier G. De; Iarossi, Dario; Menziani, Cristina; Caiolfa, Valeria; Frassineti, Chiara; Cennamo, Carlo
Journal of Medicinal Chemistry, 1987 , vol. 30, # 3 p. 459 - 464
反应条件
1: 80 percent / 85 percent m-chloroperbenzoic acid / CHCl3 / 360 h / Ambient temperature 2: 60 percent / H2 / RaNi / Ambient temperature View Scheme
参考文献
Benedetti, Pier G. De; Iarossi, Dario; Menziani, Cristina; Caiolfa, Valeria; Frassineti, Chiara; Cennamo, Carlo
Journal of Medicinal Chemistry, 1987 , vol. 30, # 3 p. 459 - 464
