2-硝基-4,5,9,10-四氢芘合成路线 (共 9 条)
反应条件
dinitrogen tetraoxide in dichloromethane 1 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 57, # 13 p. 3746 - 3748
反应条件
nitric acid in acetic acid
参考文献
Journal of Organic Chemistry, , vol. 32, p. 2272 - 2278
反应条件
nitric acid; acetic acid 1 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 54, # 2 p. 451 - 458
反应条件
1: 68 percent / triphenyltin hydride, triethylamine / acetonitrile / 1 h / Irradiation 2: 98 percent / copper(II) nitrate trihydrate / acetic anhydride / 24 h / Ambient temperature View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 106, # 4 p. 120 - 128
反应条件
1: sodium, ethanol / xylene / 1 h / 100 °C 2: 92 percent / copper(II) nitrate trihydrate / acetic anhydride / 24 h / Ambient temperature View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 107, # 1 p. 1 - 8
反应条件
1: H2 / Pd-C 2: (i) aq. HCl, NaNO2, (ii) H3PO2 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 83, p. 1974 - 1978
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene 48 h; Heating;
参考文献
Miller, Dwight W.; Herreno-Saenz, Diogenes; Huang, Kurt H.; Heinze, Thomas M.; Fu, Peter P.
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3746 - 3748
反应条件
tin(ll) chloride in acetic anhydride T=100°C; 12 h;
参考文献
Lee, Hyoyoung; Jeong, Mun Seok; Kim, Do Hyun; Zyung, Taehyoung
Patent: US2005/12092 A1, 2005 ;
Location in patent: Page 3-5; Sheet 1 ;
反应条件
1: I2 / nitrobenzene 2: N2H4*H2O / Pd-C / benzene; ethanol View Scheme
参考文献
Bolton,R.
Journal of the Chemical Society, 1964 , p. 4637 - 4638