2,5-二羟基-4'-甲基联苯合成路线 (共 8 条)
参考文献
Snam Progetti S.p.A.
Patent: US4016211 A1, 1977 ;
反应条件
tetrakis(triphenylphosphine) palladium(0); water; sodium carbonate in ethanol; toluene T=90°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Chakraborty, Mrinal; Brzozowski, Christopher F.; Novak, Michael
Journal of Physical Organic Chemistry, 2012 , vol. 25, # 12 p. 1236 - 1242
反应条件
1: sodium perchlorate; sodium bromide; acetic acid; sodium acetate / acetonitrile; water / 3 h / 30 °C / pH 4.6 2: sodium perchlorate; perchloric acid; sodium bromide / acetonitrile; water / 30 °C / pH 1 View Scheme
参考文献
Chakraborty, Mrinal; Brzozowski, Christopher F.; Novak, Michael
Journal of Physical Organic Chemistry, 2012 , vol. 25, # 12 p. 1236 - 1242
反应条件
triethylamine; PhNHN=CCIPh benzene, room temperature, 3 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Argyropoulos, N. G.; Mentzafos, D.; Terzis, A.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 7 p. 1983 - 1988
反应条件
triethylamine benzene, room temperature, 3 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Argyropoulos, N. G.; Mentzafos, D.; Terzis, A.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 7 p. 1983 - 1988
反应条件
triethylamine benzene, room temperature, 3 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Argyropoulos, N. G.; Mentzafos, D.; Terzis, A.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 7 p. 1983 - 1988
反应条件
sodium hypochlorite; tetra(n-butyl)ammonium hydrogensulfate in chloroform
0.166667 h; Ambient temperature;
参考文献
Ishii, Fumio; Kishi, Ken-ichi
Synthesis, 1980 , # 9 p. 706 - 708
反应条件
sodium hydroxide; dimethyl sulfate in water
参考文献
Polaroid Corporation
Patent: US4550214 A1, 1985 ;