5,9,14,18,23,27,32,36-八丁氧基-2,3-萘甲醛花菁合成路线 （共 3 条）
反应条件
lithium; 3,6-dibutoxy-1,2-benzene dicarbonitrile in butan-1-ol 1 h; Heating; Further byproducts given;
参考文献
Aoudia, Mohamed; Cheng, Gongzhen; Kennedy, Vance O.; Kenney, Malcolm E.; Rodgers, Michael A. J.
Journal of the American Chemical Society, 1997 , vol. 119, # 26 p. 6029 - 6039
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in butan-1-ol under Ar atm. mixt. Co(OAc)2*4H2O, naphthalocyanine, 1,8-diazabicyclo(5.4.0)undec-7-ene and 1-butanol was refluxed for 20 h; react. mixt. was diluted with MeOH and H2O, ppt. was filtered and chromed. on Al2O3-V (toluene), vac.-dried at room temp.;
参考文献
Soldatova, Alexandra V.; Kim, Junhwan; Rosa, Angela; Ricciardi, Giampaolo; Kenney, Malcolm E.; Rodgers, Michael A. J.
Inorganic Chemistry, 2008 , vol. 47, # 10 p. 4275 - 4289
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in butan-1-ol under Ar atm. soln. naphthalocyanine, 1,8-diazabicyclo(5.4.0)undec-7-eneand 1-butanol was treated with Ni(OAc)4*4H2O over 3 days; soln. was diluted with aq. MeOH and filtered, solid was chromd. on alumina (III) (toluene) and vac. dried at room temp.;
参考文献
Soldatova, Alexandra V.; Kim, Junhwan; Peng, Xinzhang; Rosa, Angela; Ricciardi, Giampaolo; Kenney, Malcolm E.; Rodgers, Michael A. J.
Inorganic Chemistry, 2007 , vol. 46, # 6 p. 2080 - 2093
