2,4,6-三异丙基苯磺胺合成路线 （共 8 条）
反应条件
ammonium hydroxide in chloroform T=20°C; 2 h;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 45 p. 6125 - 6128
反应条件
scandium tris(trifluoromethanesulfonate) in nitromethane T=50°C; 5 h;
参考文献
Synthetic Communications, , vol. 35, # 3 p. 417 - 425
反应条件
1: With N,N,N',N'',N''-pentamethyldiethylenetriamine; sec.-butyllithium in tetrahydrofuran; cyclohexane T=-78°C; 0.25 h; Inert atmosphere; 2: With chloro-trimethyl-silane in tetrahydrofuran; cyclohexane T=-78°C; 1 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 7, # 2 p. 335 - 345
反应条件
1: With N,N,N',N'',N''-pentamethyldiethylenetriamine; sec.-butyllithium in tetrahydrofuran; cyclohexane T=-78°C; 0.0166667 h; Inert atmosphere; 2: With chloro-trimethyl-silane in tetrahydrofuran; cyclohexane T=-78°C; 1 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 7, # 2 p. 335 - 345
反应条件
acetic acid; 1,1,1,3,3,3-hexamethyl-disilazane in tetrahydrofuran T=25°C; 13 h; other reagents; Product distributionMechanism;
参考文献
Journal of the American Chemical Society, , vol. 112, # 10 p. 4011 - 4030
反应条件
1: chlorosulfonic acid / dichloromethane / 0.75 h / 0 - 20 °C 2: water; ammonia / dichloromethane / 12 h / 20 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 8 p. 1505 - 1511
反应条件
sodium dithionite; cytochrome P450BM3 FLNo.62 in aq. phosphate buffer T=25°C; pH=8.0; 16 h; Inert atmosphereEnzymatic reaction; Catalytic behavior; Reagent/catalyst;
参考文献
ACS Catalysis, , vol. 4, # 2 p. 546 - 552
反应条件
in neat (no solvent)
T=160°C; 16 h;
参考文献
Han, Zhiqiang; Yang, Wenguo; Tan, Choon-Hong; Jiang, Zhiyong
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 8 p. 1505 - 1511
