反应条件
1.1: LiI / dimethylformamide / 5 h / Heating
2.1: hexamethyldisilazane / CH2Cl2 / 0.67 h / 0 - 20 °C
3.1: NaI, m-CPBA / CH2Cl2; tetrahydrofuran / 0.5 h / 0 °C
4.1: (Bu3Sn)2 / benzene / 1 h / Heating; irradiation
4.2: 87 percent / 2,2'-azobisisobutyronitrile, Bu3SnH / benzene / 1.5 h / Heating
View Scheme
参考文献
Mandville,G. et al.
Bulletin de la Societe Chimique de France, 1973 , p. 963 - 971
