1056246-70-8合成路线 （共 32 条）
反应条件
1: 83 percent / NaBH4 / ethanol; tetrahydrofuran / 25 °C
2: 96 percent / p-toluenesulfonic acid / benzene / Heating
3: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating
4: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1.1: NaBH4 / ethanol; tetrahydrofuran / 20 °C
2.1: p-TsOH / toluene / 120 °C
3.1: t-BuLi / diethyl ether / -65 °C
3.2: B(OiPr)3 / diethyl ether / 20 °C
3.3: aq. HCl / 20 °C
View Scheme
参考文献
Buettelmann, Bernd; Alanine, Alexander; Bourson, Anne; Gill, Ramanjit; Heitz, Marie-Paule; Mutel, Vincent; Pinard, Emmanuel; Trube, Gerhard; Wyler, Rene
Chimia, 2004 , vol. 58, # 9 p. 630 - 633
