1056477-06-5合成路线 （共 120 条）
反应条件
cerium(III) chloride heptahydrate in poly(ethylene glycol)-400
T=20°C; 0.5 h;
参考文献
Wu, Fang-Wen; Hou, Rei-Sheu; Wang, Huey-Min; Kang, Iou-Jiun; Chen, Ling-Ching
Heterocycles, 2011 , vol. 83, # 10 p. 2313 - 2320
反应条件
in isopropyl alcohol
1.5 h; Heating;
参考文献
Volovenko; Resnyanskaya; Tverdokhlebov
Chemistry of Heterocyclic Compounds, 2002 , vol. 38, # 3 p. 324 - 330
反应条件
bis-triphenylphosphine-palladium(II) chloride; N-benzyl-N,N,N-triethylammonium chloride; sodium acetate; triphenylphosphine
T=80°C; P=7500.6 Torr; 10 h;
参考文献
Raju, P. V. K.; Adapa, Srinivas R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 6 p. 363 - 365
反应条件
potassium carbonate; potassium iodide in acetone
18 h; Heating;
参考文献
Balakumar, Arumugham; Janardhanam, Selvasekaran; Rajagopalan, Krishnamoorthy
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 3 p. 313 - 317
反应条件
1: 2-methoxy-phenol With potassium carbonate in DMF (N,N-dimethyl-formamide)
T=140°C; 1 - 2 h;
2: 2-bromo-cyclo-hexanone in DMF (N,N-dimethyl-formamide)
T=20°C; 24 h;
参考文献
GLENMARK PHARMACEUTICALS LTD.; BALASUBRAMANIAN, Gopalan; GHARAT, Laxmikant, Atmaram; LAKDAWALA, Aftab, Dawoodbhai; BEDEKAR, Sarika, Suhas
Patent: WO2004/69831 A1, 2004 ;
Location in patent: Page 28-29 ;
WO 2004/069831 A1
参考文献
Mitra et al.
Current Science, 1954 , vol. 23, p. 263
反应条件
ammonium hydroxide
T=120°C; 0.333333 h; microwave irradiation;
参考文献
Utsukihara, Takamitsu; Nakamura, Hiroaki; Watanabe, Masashige; Akira Horiuchi
Tetrahedron Letters, 2006 , vol. 47, # 52 p. 9359 - 9364
反应条件
in toluene
T=20°C; 0.25 h;
参考文献
Conti, Irene; Marchioni, Filippo; Credi, Alberto; Orlandi, Giorgio; Rosini, Goffredo; Garavelli, Marco
Journal of the American Chemical Society, 2007 , vol. 129, # 11 p. 3198 - 3210
反应条件
1: 73 percent / p-toluanesulfonic acid / benzene / 12 h / Heating
2: 79 percent / Li / diethyl ether / 5.5 h / 40 - 45 °C
3: Adams catalyst / diethyl ether
View Scheme
参考文献
Ferber, Peter H.; Gream, George E.; Stoneman, Terry I.
Australian Journal of Chemistry, 1985 , vol. 38, # 5 p. 699 - 711
参考文献
Cristol; Rademacher
Journal of the American Chemical Society, 1959 , vol. 81, p. 1600
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Winstein
Journal of the American Chemical Society, 1939 , vol. 61, p. 1610
