1056477-06-5合成路线 （共 120 条）
反应条件
in ethanol Hantzsch type reaction; 6 h; Reflux;
参考文献
Lang, Martin; Seifert, Markus H.-J.; Wolf, Kristina K.; Aschenbrenner, Andrea; Baumgartner, Roland; Wieber, Tanja; Trentinaglia, Viola; Blisse, Marcus; Tajima, Nobumitsu; Yamashita, Tokuyuki; Vitt, Daniel; Noda, Hitoshi
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 18 p. 5417 - 5422
反应条件
1: 85 percent / NaOH / aq. ethanol / r.t., 30min., then reflux, 4h 2: 84 percent / polyphosphoric acid / 1.5 h / 190 - 200 °C 3: 63 percent / Se powder / 8 h / 300 °C View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1485 - 1495
反应条件
1: aniline; diethyl ether 2: methanol; hydroxylamine 3: alcohol; sodium View Scheme
参考文献
Koetz; Grethe
Journal fuer Praktische Chemie (Leipzig), 1909 , vol. <2> 80, p. 488
反应条件
1: 0.23 h / 20 °C / |Ionic liquid 2: sodium cyanoborohydride; acetic acid / 36 h / 20 °C 3: hydrazine hydrate / water / 3 h / 60 °C View Scheme
参考文献
Gupta, Pankaj; Rouf, Abdul; Shah, Bhahwal A.; Mukherjee, Debaraj; Taneja, Subhash C.
Synthetic Communications, 2013 , vol. 43, # 4 p. 505 - 519
反应条件
in 2-ethoxy-ethanol Bischler reaction; 0.166667 h; microwave irradiation;
参考文献
Chen, Jing; Hu, Yongzhou
Synthetic Communications, 2006 , vol. 36, # 11 p. 1485 - 1494
反应条件
water; sodium chloride T=100°C; 0.25 h; microwave irradiation;
参考文献
Tetrahedron Letters, , vol. 47, # 52 p. 9359 - 9364
反应条件
1: 0.23 h / 20 °C / |Ionic liquid 2: sodium cyanoborohydride; acetic acid / 36 h / 20 °C 3: hydrazine hydrate / water / 3 h / 60 °C View Scheme
参考文献
Gupta, Pankaj; Rouf, Abdul; Shah, Bhahwal A.; Mukherjee, Debaraj; Taneja, Subhash C.
Synthetic Communications, 2013 , vol. 43, # 4 p. 505 - 519
反应条件
cerium(III) iodide in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Fukuzawa, Shin-ichi; Tsuruta, Takuya; Fujinami, Tatsuo; Sakai, Shizuyoshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1473 - 1478
反应条件
cerium(IV) sulphate; oxygen T=50°C; Oxidation; 6 h;
参考文献
He, Liangyou; Horiuchi, C. Akira
Bulletin of the Chemical Society of Japan, 1999 , vol. 72, # 11 p. 2515 - 2521
反应条件
1: 0.23 h / 20 °C / |Ionic liquid 2: sodium cyanoborohydride; acetic acid / 36 h / 20 °C 3: hydrazine hydrate / water / 3 h / 60 °C View Scheme
参考文献
Gupta, Pankaj; Rouf, Abdul; Shah, Bhahwal A.; Mukherjee, Debaraj; Taneja, Subhash C.
Synthetic Communications, 2013 , vol. 43, # 4 p. 505 - 519
