2-氨基-1-甲基-6-苯基咪唑[4,5-b]吡啶合成路线 (共 35 条)
反应条件
1: With phosphorus pentachloride 2: With ammonia
参考文献
Bergman, Jan
Tetrahedron Letters, 2009 , vol. 50, # 40 p. 5631 - 5632
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in 1,4-dioxane; water T=120°C; Suzuki Coupling; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Journal of the Korean Chemical Society, , vol. 57, # 3 p. 361 - 364
反应条件
N,O-bis-(trimethylsilyl)-acetamide T=120°C; 2 h;
参考文献
Lindstroem
Acta chemica Scandinavica (Copenhagen, Denmark : 1989), 1995 , vol. 49, # 5 p. 361 - 363
反应条件
1: pyridine / Heating 2: K2CO3 / acetone / Ambient temperature 3: 68 percent / I2 / H2O; acetic acid / 80 °C 4: 45 percent / trifluoroacetic acid / 2 h / Irradiation 5: Heating 6: 80 percent / NaNH2 View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 44 p. 7793 - 7796
反应条件
1: K2CO3 / acetone / Ambient temperature 2: 68 percent / I2 / H2O; acetic acid / 80 °C 3: 45 percent / trifluoroacetic acid / 2 h / Irradiation 4: Heating 5: 80 percent / NaNH2 View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 44 p. 7793 - 7796
反应条件
1: 68 percent / I2 / H2O; acetic acid / 80 °C 2: 45 percent / trifluoroacetic acid / 2 h / Irradiation 3: Heating 4: 80 percent / NaNH2 View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 44 p. 7793 - 7796
反应条件
1: 45 percent / trifluoroacetic acid / 2 h / Irradiation 2: Heating 3: 80 percent / NaNH2 View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 44 p. 7793 - 7796
反应条件
1: 58 percent / NaNH2 / toluene 2: 3.1 g / Br2 / acetic acid / 1 h / Ambient temperature 3: CuSO4 / H2O / 72 h / 200 °C / Heating 4: ethanol / 1 h / 175 °C View Scheme
参考文献
Heterocycles, , vol. 24, # 7 p. 1815 - 1819
反应条件
1: 3.1 g / Br2 / acetic acid / 1 h / Ambient temperature 2: CuSO4 / H2O / 72 h / 200 °C / Heating 3: ethanol / 1 h / 175 °C View Scheme
参考文献
Heterocycles, , vol. 24, # 7 p. 1815 - 1819
反应条件
1: CuSO4 / H2O / 72 h / 200 °C / Heating 2: ethanol / 1 h / 175 °C View Scheme
参考文献
Heterocycles, , vol. 24, # 7 p. 1815 - 1819