反应条件
Multi-step reaction with 3 steps 1: 80 percent / PCl5 / diethyl ether / 0.5 h / 0 °C2: 1) bis(trimethylsilyl)acetamide / 1) CH2Cl2, 0 deg C, 30 min, 2) CH2Cl2, 0 deg C, then 25 deg C, 3 h3: NaHCO3 / methanol; H2O / 2 h / Irradiation
参考文献
Raucher, Stanley; Bray, Brian L.; Lawrence, Ross F. Journal of the American Chemical Society, 1987 , vol. 109, # 2 p. 442 - 446
