2,4-二甲基-1,3-环己二烯-1-羧酸合成路线 （共 2 条）
反应条件
aluminum tri-bromide in tetramethylene sulfide 4.5 h; Ambient temperature;
参考文献
Kawasaki, Motoji; Matsuda, Fuyuhiko; Terashima, Shiro
Tetrahedron, 1988 , vol. 44, # 18 p. 5727 - 5744
反应条件
1: 1.) LDA / 1.) THF, -60 deg C, 2.) THF, r.t.
2: 85 percent / tetrahydrofuran / 0.5 h / Ambient temperature
3: 85 percent / DDQ, CSA / benzene / 5 h / Heating
4: 87 percent / 1N HCl / 12 h / Heating
View Scheme
参考文献
Kawasaki, Motoji; Matsuda, Fuyuhiko; Terashima, Shiro
Tetrahedron, 1988 , vol. 44, # 18 p. 5727 - 5744
