反应条件
lithium perchlorate; trifluoroacetic anhydride 2.) DMF, water, 0.3 M LiClO4, electrolysis, cell with glass diaphragm, base mercury as cathode, platinum mesh as anode, saturated calomel electrode as reference, controlled potential, E=-1.1 to -1.2 V, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Veselovskii, V. V.; Novikova, M. A.; Korotaeva, L. M.; Dragan, V. A.; Gul'tyai, V. P.; Moiseenkov, A. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 8.2 p. 1722 - 1724
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 8 p. 1895 - 1896