3-溴-3,3-二氟丙酸乙酯合成路线 （共 6 条）
反应条件
oxone in ethanol T=20°C; Oxidation; 24 h;
参考文献
Peng, Sheng; Qing, Feng-Ling; Li, Yi-Qun; Hu, Chang-Ming
Journal of Organic Chemistry, 2000 , vol. 65, # 3 p. 694 - 700
反应条件
1: 1 h / 0 °C 2: 75 percent / Caro's acid / ethanol / 1.) 5-10 deg C; 2.) room temperature, 1 day View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 37, p. 183 - 190
反应条件
2: 68 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0 °C View Scheme
参考文献
Molines, H.; Wakselman, C.
Journal of Fluorine Chemistry, 1987 , vol. 37, p. 183 - 190
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=0°C;
参考文献
Molines, H.; Wakselman, C.
Journal of Fluorine Chemistry, 1987 , vol. 37, p. 183 - 190
反应条件
triethylamine in N,N-dimethyl-formamide T=70°C; 3 h; SolventReagent/catalystTemperature;
参考文献
Ou, Song; Jiang, Min; Liu, Jin-Tao
Tetrahedron, 2013 , vol. 69, # 51 p. 10820 - 10825
反应条件
hydrogen bromide T=70°C;
参考文献
McNaughton, Don; Elmes, Patricia
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1992 , vol. 48, # 4 p. 605 - 612
