N-BOC-O-甲苯磺酰羟胺合成路线 （共 18 条）
反应条件
triethylamine in benzene T=0°C; 1 h;
参考文献
Greck, Christine; Bischoff, Laurent; Girard, Anne; Hajicek, Josef; Genet, Jean-Pierre
Bulletin de la Societe Chimique de France, 1994 , vol. 131, # 4 p. 429 - 433
反应条件
1: water; hydroxylamine hydrochloride / anschliessend mit wss. Natronlauge View Scheme
参考文献
Carpino et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 955
反应条件
1: aqueous acetic acid; sodium nitrite 2: water; hydroxylamine hydrochloride / anschliessend mit wss. Natronlauge View Scheme
参考文献
Carpino et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 955
反应条件
1: hydroxylamine; sodium hydrogencarbonate / methanol; water 2: 4-methyl-morpholine / dichloromethane / 0 - 20 °C View Scheme
参考文献
Molnar, Istvan Gabor; Tanzer, Eva-Maria; Daniliuc, Constantin; Gilmour, Ryan
Chemistry - A European Journal, 2014 , vol. 20, # 3 p. 794 - 800
反应条件
4-methyl-morpholine in dichloromethane T=10 - 20°C; 18 h;
参考文献
Baburaj, Thankappan; Thambidurai, Sivalingam
Synlett, 2011 , # 14 art. no. B08111ST, p. 1993 - 1996
反应条件
copper(l) iodide; n-butyllithium 1.) -78 deg C, 1 h; 2.) 0 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Greck, Christine; Bischoff, Laurent; Girard, Anne; Hajicek, Josef; Genet, Jean-Pierre
Bulletin de la Societe Chimique de France, 1994 , vol. 131, # 4 p. 429 - 433
反应条件
n-butyllithium 1.) -78 deg C, 1 h; 2.) -78 - -40 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Genet; Mallart; Greck; Piveteau
Tetrahedron Letters, 1991 , vol. 32, # 21 p. 2359 - 2362
反应条件
4-methyl-morpholine in dichloromethane T=10 - 20°C; 18 h;
参考文献
Baburaj, Thankappan; Thambidurai, Sivalingam
Synlett, 2011 , # 14 art. no. B08111ST, p. 1993 - 1996
反应条件
potassium carbonate; dirhodium(II) terakis(triphenylacetate) in dichloromethane
T=25°C;
参考文献
Lebel, Helene; Kim, Huard
Organic Letters, 2007 , vol. 9, # 4 p. 639 - 642
反应条件
potassium carbonate; dirhodium(II) terakis(triphenylacetate) in dichloromethane
T=25°C;
参考文献
Lebel, Helene; Kim, Huard
Organic Letters, 2007 , vol. 9, # 4 p. 639 - 642
