N-BOC-O-甲苯磺酰羟胺合成路线 （共 18 条）
反应条件
Rh2(triphenylacetate)4; potassium carbonate in dichloromethane
T=25°C; 6 h;
参考文献
Huard, Kim; Lebel, Helene
Chemistry - A European Journal, 2008 , vol. 14, # 20 p. 6222 - 6230
反应条件
K2OsO4*2H2O; water in tert-butyl alcohol
T=0 - 20°C; regioselective reaction;
参考文献
Masruri; Willis, Anthony C.; McLeod, Malcolm D.
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8480 - 8491
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=10 - 20°C; 16 h;
参考文献
Baburaj, Thankappan; Thambidurai, Sivalingam
Synlett, 2011 , # 14 art. no. B08111ST, p. 1993 - 1996
反应条件
4-methyl-morpholine in dichloromethane
T=10 - 20°C; 18 h;
参考文献
Baburaj, Thankappan; Thambidurai, Sivalingam
Synlett, 2011 , # 14 art. no. B08111ST, p. 1993 - 1996
反应条件
in tetrahydrofuran
T=-78 - -40°C; 3 h;
参考文献
Genet; Mallart; Greck; Piveteau
Tetrahedron Letters, 1991 , vol. 32, # 21 p. 2359 - 2362
反应条件
n-butyl-magnesium chloride
1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 1.5 h; Yield given. Multistep reaction;
参考文献
Greck, Christine; Bischoff, Laurent; Girard, Anne; Hajicek, Josef; Genet, Jean-Pierre
Bulletin de la Societe Chimique de France, 1994 , vol. 131, # 4 p. 429 - 433
反应条件
4-methyl-morpholine in dichloromethane
T=10 - 20°C; 18 h;
参考文献
Baburaj, Thankappan; Thambidurai, Sivalingam
Synlett, 2011 , # 14 art. no. B08111ST, p. 1993 - 1996
反应条件
4-methyl-morpholine in dichloromethane
T=10 - 20°C; 18 h;
参考文献
Baburaj, Thankappan; Thambidurai, Sivalingam
Synlett, 2011 , # 14 art. no. B08111ST, p. 1993 - 1996
