反应条件
1: 1.) NaH / 1.) dioxane, MeOH, reflux; 2.) reflux, 90 min 2: 62 percent / 1.) KOH / methanol; H2O / 2 h / Heating 3: OsO4, NaIO4 / diethyl ether; H2O 4: LAH / diethyl ether 5: 1.) pyridine; 2.) 6N HCl aq. View Scheme
参考文献
Kitahara, Takeshi; Mori, Masataka; Koseki, Koshi; Mori, Kenji
Tetrahedron Letters, 1986 , vol. 27, # 12 p. 1343 - 1346
