sulfuric acid; iodine; iodic acid in water; acetic acid

sulfuric acid; 4'-methylpropiophenone; trimethyl orthoformate T=60°C; 2 h;

thermolysis Product distributionMechanism;

thermolysis; Product distributionMechanism;

pyridine; palladium diacetate; potassium carbonate T=100°C; 3 h; Ionic liquid;

暂无反应条件数据

1.1: 80 percent / 1,10-phenanthroline; cuprous chloride; potassium hydroxide / toluene / 5 h / 125 °C 2.1: n-butyllithium / diethyl ether; cyclohexane / 1 h / 20 °C 2.2: iodine / diethyl ether; cyclohexane / 0 °C View Scheme

palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; sodium t-butanolate in anhydrous xylene T=120°C; 2 h; Inert atmosphere;

1: copper / dimethyl sulfoxide / 12 h / 60 °C / |Inert atmosphere 2: potassium carbonate / methanol; water / 2 h / 20 °C / |Inert atmosphere 3: 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); silver nitrate / water; acetone / 1 h / 55 °C / |Inert atmosphere; |Schlenk technique View Scheme