单溴亚甲基二膦酸四异丙基酯合成路线 （共 3 条）
反应条件
tin(ll) chloride in ethanol; water 0.166667 h;
参考文献
McKenna, Charles E.; Khawli, Leslie A.; Ahmad, Wan-Yaacob; Pham, Phuong; Bongartz, Jean-Pierre
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 37, p. 1 - 12
反应条件
1: With sodium hydride in toluene T=20°C; 1.5 h; 2: With bromine in dichloromethane; toluene T=0 - 5°C; 3.5 h;
参考文献
Nuretdinov, I. A.; Gubskaya, V. P.; Shishikina, N. I.; Fazleeva, G. M.; Berezhnaya, L. Sh.; Karaseva, I. P.; Sibgatullina, F. G.; Zverev, V. V.
Russian Chemical Bulletin, 2002 , vol. 51, # 2 p. 337 - 341
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 2002 , # 2 p. 317 - 320
反应条件
2: Br2, aq. K2CO3 / heptane View Scheme
参考文献
Quimby,O.T. et al.
Journal of Organometallic Chemistry, 1968 , vol. 13, p. 199 - 207
