反应条件
Multi-step reaction with 2 steps 1: 1.) butyl-lithium, di-isopropylamine, 2.) water / 1.) THF, hexane, 2.) THF, hexane2: 1.) LDA / 1.) THF, -78 to -40 deg C, 1.5 h then -40 deg C, 30 min, 2.) THF, -78 deg C
参考文献
Dziadulewicz, Edward; Hodgson, David; Gallagher, Timothy Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3367 - 3374