反应条件
1: N-ethyl-N,N-diisopropylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 0.5 h / -15 °C / |Inert atmosphere
2: CjNCS2 / acetonitrile / 3 h / 37 °C / pH 7.4 / |Enzymatic reaction
View Scheme
参考文献
Pesnot, Thomas; Gershater, Markus C.; Ward, John M.; Hailes, Helen C.
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 16 p. 2997 - 3008