3-乙酰基-2,5-二甲基呋喃合成路线 （共 22 条）
反应条件
1: 46 percent / Mn(OAc)2, O2, AcOH / 23 °C 2: 81 percent / HClO4 / acetonitrile / 0.25 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 31, # 5 p. 1219 - 1228
反应条件
sodium acetate; zinc(II) chloride T=200 - 205°C; im Autoklaven;
参考文献
Gazzetta Chimica Italiana, , vol. 24 I, p. 436
反应条件
diethyl sodium phosphite in benzene Reduction; oxidation; 4 h; Heating; Title compound not separated from byproducts;
参考文献
Russian Journal of General Chemistry, , vol. 66, # 5 p. 743 - 749
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 474 - 480
Zhurnal Organicheskoi Khimii, , vol. 19, # 3 p. 541 - 548
反应条件
alkaline aqueous potassium hypochlorite solution
参考文献
Hurd; Wilkinson
Journal of the American Chemical Society, 1948 , vol. 70, p. 739
反应条件
diethyl ether; sodium methylate
参考文献
Barkley; Levine
Journal of the American Chemical Society, 1951 , vol. 73, p. 4625
反应条件
copper(ll) bromide in chloroform; ethyl acetate 2.5 h; Heating / reflux;
参考文献
PHARMACIA and UPJOHN COMPANY
Patent: WO2004/106345 A2, 2004 ;
Location in patent: Page 46 ;
反应条件
bromine in 1,4-dioxane; diethyl ether
参考文献
Strohbach, Joseph Walter; Tanis, Steven P.; Moon, Malcolm Wilson; Nieman, James A.; Beauchamp, Thomas J.; Northuis, Jill M.; McGhee, William D.
Patent: US2003/207877 A1, 2003 ;
反应条件
ammonia T=110 - 115°C;
参考文献
Magnanini; Bentivoglio
Gazzetta Chimica Italiana, 1894 , vol. 24 I, p. 436
参考文献
Magnanini; Bentivoglio
Gazzetta Chimica Italiana, 1894 , vol. 24 I, p. 436
