3,7-二甲基-1-辛醇合成路线 (共 89 条)
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; Catalytic hydrogenation; 24 h;
参考文献
Sajiki, Hironao; Hirota, Kosaku
Tetrahedron, 1998 , vol. 54, # 46 p. 13981 - 13996
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; desilylation; 24 h;
参考文献
Hattori, Kazuyuki; Sajiki, Hironao; Hirota, Kosaku
Tetrahedron Letters, 2000 , vol. 41, # 30 p. 5711 - 5714
反应条件
polymeric xylylene-ionene borohydride in methanol T=20°C; 0.5 h;
参考文献
Lakouraj, Moslem M.; Tajbakhsh, Mahmood; Mahalli, Majid S.
Monatshefte fur Chemie, 2008 , vol. 139, # 2 p. 117 - 123
反应条件
hydrogen in tert-butyl alcohol T=80°C; P=1500.15 - 15001.5 Torr; 8 h; Autoclave; diastereoselective reaction;
参考文献
Nie, Yuntong; Jaenicke, Stephan; Chuah, Gaik-Khuan
Chemistry - A European Journal, 2009 , vol. 15, # 8 p. 1991 - 1999
反应条件
palladium 10 on activated carbon; sodium formate in toluene T=80°C; 0.5 h; Microwave irradiationSealed tube; Reagent/catalystSolvent;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 366, p. 315 - 320
反应条件
hydrogen in tert-butyl alcohol T=80°C; P=7500.75 Torr; 8 h; Autoclave; diastereoselective reaction;
参考文献
Nie, Yuntong; Jaenicke, Stephan; Chuah, Gaik-Khuan
Chemistry - A European Journal, 2009 , vol. 15, # 8 p. 1991 - 1999
反应条件
palladium 10 on activated carbon; sodium formate in water; toluene T=80°C; 0.5 h; Microwave irradiationSealed tube; Reagent/catalystSolvent;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 366, p. 315 - 320
反应条件
lithium aluminium tetrahydride in diethyl ether T=20°C;
参考文献
Journal of the American Chemical Society, , vol. 125, # 1 p. 158 - 162
反应条件
hydrogen; palladium on activated charcoal in methanol P=760.051 Torr; Title compound not separated from byproducts.;
参考文献
Chemical Communications, , # 12 p. 1325 - 1327
反应条件
1: H2 / Pd/C 2: LiAlH4 / diethyl ether / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 1 p. 158 - 162