3,7-二甲基-1-辛醇合成路线 （共 89 条）
反应条件
1.1: 81 percent / LiI / dimethylformamide / 12 h / Heating 2.1: n-BuLi / tetrahydrofuran; hexane / 1 h / 20 °C 2.2: 85 percent / tetrahydrofuran; hexane / 0 - 20 °C 3.1: 90 percent / KOH / methanol / 4 h / Heating 4.1: H2 / Pd/C / methanol / 5 h View Scheme
参考文献
Chemistry of Natural Compounds, , vol. 37, # 5 p. 486 - 489
反应条件
1: aq. H2SO4 2: H2 / Raney-Ni / methanol View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 679, p. 26 - 34
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 1.) -10 deg C 2.) RT;
参考文献
Tetrahedron, , vol. 42, # 18 p. 5003 - 5010
反应条件
ethanol; palladium 10 on activated carbon T=20°C; 2 h;
参考文献
Banerjee, Subhash; Balasanthiran, Vagulejan; Koodali, Ranjit T.; Sereda, Grigoriy A.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 19 p. 4316 - 4321
反应条件
hydrogen; Zr-beta and 15percentNi/MCM-41 in tert-butyl alcohol T=80°C; P=15001.5 Torr; 1 h; Product distribution; Further Variations:Catalysts;
参考文献
Journal of Catalysis, , vol. 248, # 1 p. 1 - 10
反应条件
1: 82 percent / pyridine / 72 h / 0 °C 2: 82 percent / lithium aluminium hydride / tetrahydrofuran / 1.) -10 deg C 2.) RT View Scheme
参考文献
Tetrahedron, , vol. 42, # 18 p. 5003 - 5010
反应条件
hydrogen; Pt/Al2O3; octane-1-acetic acid in hexane T=0°C; variation of catalyst; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 12 p. 3779 - 3782
反应条件
Pd/C/TiO2; hydrogen T=89.84°C; P=22502.3 Torr; Autoclave;
参考文献
Chinese Journal of Chemistry, , vol. 29, # 4 p. 655 - 660
反应条件
1: oxalic acid, benzene-1,4-diol / H2O / Heating 2: (i) H2, Raney-Ni, MeOH, (ii) H2, Pd-C View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 679, p. 26 - 34
反应条件
Pt(5wt)Sn(1wt)/Al2O3; hydrogen in isopropyl alcohol T=70°C; P=760.051 Torr; 2 h; Activation energyKinetics; Reagent/catalyst;
参考文献
Applied Catalysis A: General, , vol. 392, # 1-2 p. 208 - 217
