3,7-二甲基-1-辛醇合成路线 （共 89 条）
反应条件
1: 92 percent / CCL / diethyl ether / 16 h / 20 - 22 °C
2: 91 percent / KOH / methanol / 1.5 h / 20 - 22 °C
View Scheme
参考文献
Gamalevich; Serebryakov
Russian Chemical Bulletin, 1997 , vol. 46, # 1 p. 171 - 183
反应条件
1: 84 percent / pyridine / 20 °C
2: 56 percent / K2CO3 / dimethylformamide / 80 °C
3: 81 percent / HNO3; H2SO4 / CH2Cl2 / 1.5 h / 20 °C
View Scheme
参考文献
Grolik, Jaroslaw; Sieron, Leslaw; Eilmes, Julita
Tetrahedron Letters, 2006 , vol. 47, # 47 p. 8209 - 8213
反应条件
sulfuric acid in cyclohexane
5 h; Heating;
参考文献
Hanif, Raja Muhammad; Qineng, Ping; Fenzhu, Muo
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 9 p. 1428 - 1431
参考文献
Cambou, Bernard; Klibanov, Alexander M.
Journal of the American Chemical Society, 1984 , vol. 106, # 9 p. 2687 - 2692
参考文献
Grolik, Jaroslaw; Sieron, Leslaw; Eilmes, Julita
Tetrahedron Letters, 2006 , vol. 47, # 47 p. 8209 - 8213
参考文献
Natelson; Gottfried; Kornblau
Journal of the American Chemical Society, 1942 , vol. 64, p. 1484
反应条件
Oxonereg;; 2-iodo benzoic acid; tetra(n-butyl)ammonium hydrogensulfate in ethyl acetate
T=70°C; 7 h;
参考文献
Schulze, Agnes; Giannis, Athanassios
Synthesis, 2006 , # 2 art. no. P09505SS, p. 257 - 260
反应条件
potassium dichromate; sulfuric acid
参考文献
Schulze, Agnes; Pagona, Georgia; Giannis, Athanassios
Synthetic Communications, 2006 , vol. 36, # 9 p. 1147 - 1156
反应条件
pyridine; thionyl chloride
参考文献
Smith et al.
Journal of Organic Chemistry, 1939 , vol. 4, p. 340
