thionyl chloride; triethylamine in diethyl ether 12 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ogura, Katsuyuki; Sanada, Kunio; Takahashi, Kazumasa; Iida, Hirotada
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 83 - 88
triphenylphosphine hydrochloride; N,N-dimethyl-formamide anschliessend mit 2,6,11,15-Tetramethyl-hexadeca-2t,4t,6t,8t,10t,12t,14t-heptaendial dann mit methanol. Natriummethylat;
参考文献
Fontan, Noelia; Vaz, Belen; Alvarez, Rosana; De Lera, Angel R.
Chemical Communications, 2013 , vol. 49, # 26 p. 2694 - 2696