1: dichloromethane / 0.5 h / 0 °C
2: methanol; potassium carbonate / water / 3 h / 20 °C
3: carbon tetrabromide; triethylamine; triphenylphosphine / dichloromethane / 0.5 h / -10 °C
View Scheme
参考文献
Ichikawa, Yoshiyasu; Osada, Masafumi; Ohtani, Ikuko I.; Isobe, Minoru
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 10 p. 1449 - 1455
1: With caesium carbonate; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in 1,3,5-trimethyl-benzene
T=100°C; 3 h;
2: With triphenyl phosphite in 1,3,5-trimethyl-benzene
T=150°C; 15 h;
参考文献
Morita, Masao; Sakaguchi, Satoshi; Ishii, Yasutaka
Journal of Organic Chemistry, 2006 , vol. 71, # 16 p. 6285 - 6286