sodium hydroxide; tributoxyborane; dihydrogen peroxide; magnesium 1) THF, 25 deg C --> reflux (40 min), reflux (1 h); 2) 0 - 5 deg C, THF; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, # 2 p. 285 - 290
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 2 p. 365 - 371